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  <doc>
    <id>60289</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>lecture</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Diffraction and Single-Crystal Elastic Constants of Laser Powder Bed Fused Inconel 718</title>
    <abstract language="eng">Laser powder bed fusion (PBF-LB/M) of metallic alloys is a layer-wise additive manufacturing process that provides significant scope for more efficient designs of components, benefiting performance and weight, leading to efficiency improvements for various sectors of industry. However, to benefit from these design freedoms, knowledge of the high produced induced residual stress and mechanical property anisotropy associated with the unique microstructures is critical. X-ray and neutron diffraction are considered the benchmark for non-destructive characterization of surface and bulk internal residual stress. The latter, characterized by the high penetration power in most engineering alloys, allows for the use of a diffraction angle close to 90° enabling a near cubic sampling volume to be specified. However, the complex microstructures of columnar growth with inherent crystallographic texture typically produced during PBF-LB/M of metallics present significant challenges to the assumptions typically required for time efficient determination of residual stress. These challenges include the selection of an appropriate set of diffraction elastic constants and a representative lattice plane suitable for residual stress analysis. In this contribution, the selection of a suitable lattice plane family for residual stress analysis is explored. Furthermore, the determination of an appropriate set of diffraction and single-crystal elastic constants depending on the underlying microstructure is addressed.&#13;
In-situ loading experiments have been performed at the Swiss Spallation Neutron Source with the main scope to study the deformation behaviour of laser powder bed fused Inconel 718. Cylindrical tensile bars have been subjected to an increasing mechanical load. At pre-defined steps, neutron diffraction data has been collected. After reaching the yield limit, unloads have been performed to study the accumulation of intergranular strain among various lattice plane families.</abstract>
    <enrichment key="eventName">11th European Conference on Residual Stresses</enrichment>
    <enrichment key="eventPlace">Prag, Czech Republic</enrichment>
    <enrichment key="eventStart">03.06.2024</enrichment>
    <enrichment key="eventEnd">07.06.2024</enrichment>
    <enrichment key="InvitedTalks">0</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
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    <author>Jakob Schröder</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Additive Manufacturing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Laser Powder Bed fusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffraction Elastic Constants</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Microstructure</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electron Backscatter Diffraction</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.6 Additive Fertigung metallischer Komponenten</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
  </doc>
  <doc>
    <id>59900</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>lecture</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Diffraction and Single-Crystal Elastic Constants of Laser Powder Bed Fused Inconel 718</title>
    <abstract language="eng">In this presentation, the results of the determination of the diffraction and single-crystal elastic constants of laser powder bed fused Inconel 718 are presented. The analysis is based on high-energy synchrotron diffraction experiments performed at the Deutsches Elektronen-Synchrotron. It is shown that the characteristic microstructure of laser powder bed fused Inconel 718 impacts the elastic anisotropy and therefore the diffraction and single-crystal elastic constants. Finally, the consequences on the diffraction-based residual stress determination of laser powder bed fused Inconel 718 are discussed.</abstract>
    <enrichment key="eventName">AWT-Fachausschuss 13 "Eigenspannungen"</enrichment>
    <enrichment key="eventPlace">Wolfsburg, Germany</enrichment>
    <enrichment key="eventStart">19.03.2024</enrichment>
    <enrichment key="eventEnd">20.03.2024</enrichment>
    <enrichment key="RelatedIdentifier">https://doi.org/10.1016/j.matlet.2023.135305</enrichment>
    <enrichment key="InvitedTalks">0</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <author>Jakob Schröder</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Additive Manufacturing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Laser Powder Bed fusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>In-Situ Testing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffraction Elastic Constants</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.6 Additive Fertigung metallischer Komponenten</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
  </doc>
  <doc>
    <id>65213</id>
    <completedYear/>
    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>9726</pageFirst>
    <pageLast>9737</pageLast>
    <pageNumber/>
    <edition/>
    <issue>12</issue>
    <volume>77</volume>
    <type>article</type>
    <publisherName>Springer Nature</publisherName>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Resolving the Subsurface Residual Stress Maximum in Laser Powder Bed-Fused 316L Stainless Steel by Diffraction-Based Analysis</title>
    <abstract language="eng">Laser powder bed fusion (PBF-LB/M) is a metal additive manufacturing process. Due to the complex nature of the layer-wise, repeated heating and cooling cycles, it tends to generate high-magnitude residual stresses. If not correctly understood and mitigated through in- or post-process approaches, these residual stresses can be detrimental as they are often tensile at the surface. However, determining the magnitude and location of peak tensile residual stresses is not trivial as they are often located subsurface. This work focuses on determining the magnitude and location of these deleterious tensile residual stresses in a PBF-LB/316L specimen. Two diffraction-based Methods are used to reveal the relationship between the residual stresses and the underlying microstructure. On the one hand, high spatial resolution Neutron diffraction is used to determine triaxial stresses from the bulk to a depth of 0.15 mm. On the other hand, laboratory X-ray diffraction coupled with electrolytical layer removal allows the biaxial residual stress depth profile to be probed from the surface to a depth of about 0.6 mm. The results show a good agreement between the two methods. The peak residual stress is shown to be 500 MPa, which appears as a plateau between 0.08 and 0.35 mm in depth.</abstract>
    <parentTitle language="eng">JOM - The Journal of The Minerals, Metals &amp; Materials Society (TMS)</parentTitle>
    <identifier type="doi">10.1007/s11837-025-07719-y</identifier>
    <identifier type="issn">1543-1851</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-652138</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">22.12.2025</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Alexander Evans</author>
    <author>Jakob Schröder</author>
    <author>T. Pirling</author>
    <author>Alexander Ulbricht</author>
    <author>Patricia Suárez Ocaño</author>
    <author>Giovanni Bruno</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Residual stress</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Laser Powder Bed Fusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>316L</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Additive manufacturing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Microstructure</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>AGIL</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/65213/Evans_JOM_2025.pdf</file>
  </doc>
  <doc>
    <id>55584</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>15036</pageFirst>
    <pageLast>15058</pageLast>
    <pageNumber/>
    <edition/>
    <issue>57</issue>
    <volume>2022</volume>
    <type>article</type>
    <publisherName>Springer Science + Business Media B.V.</publisherName>
    <publisherPlace>Dordrecht</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Understanding the impact of texture on the micromechanical anisotropy of laser powder bed fused Inconel 718</title>
    <abstract language="eng">The manufacturability of metallic alloys using laser-based additive manufacturing methods such as laser powder bed fusion has substantially improved within the last decade. However, local melting and solidification cause hierarchically structured and crystallographically textured microstructures possessing large residual stress. Such microstructures are not only the origin of mechanical anisotropy but also pose metrological challenges for the diffraction-based residual stress determination. Here we demonstrate the influence of the build orientation and the texture on the microstructure and consequently the mechanical anisotropy of as-built Inconel 718. For this purpose, we manufactured specimens with [001]/[011]-, [001]- and [011]/[111]-type textures along their loading direction. In addition to changes in the Young’s moduli, the differences in the crystallographic textures result in variations of the yield and ultimate tensile strengths. With this in mind, we studied the anisotropy on the micromechanical scale by subjecting the specimens to tensile loads along the different texture directions during in situ neutron diffraction experiments. In this context, the response of multiple lattice planes up to a tensile strain of 10% displayed differences in the load partitioning and the residual strain accumulation for the specimen with [011]/[111]-type texture. However, the relative behavior of the specimens possessing an [001]/[011]- and [001]-type texture remained qualitatively similar. The consequences on the metrology of residual stress determination methods are discussed.</abstract>
    <parentTitle language="eng">Journal of materials science</parentTitle>
    <identifier type="doi">10.1007/s10853-022-07499-9</identifier>
    <identifier type="issn">1573-4803</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-555840</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">29.08.2022</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Jakob Schröder</author>
    <author>Alexander Evans</author>
    <author>E. Polatidis</author>
    <author>J. Čapek</author>
    <author>Gunther Mohr</author>
    <author>Itziar Serrano-Munoz</author>
    <author>Giovanni Bruno</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Laser powder bed fusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Additive manufacturing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electron backscatter diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Tensile testing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffraction</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <collection role="institutes" number="">9.6 Additive Fertigung metallischer Komponenten</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/55584/Understanding the impact of texture on the micromechanical anisotropy of L-PBF Inconel 718.pdf</file>
  </doc>
  <doc>
    <id>56376</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>lecture</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Texture Dependent Micromechanical Anisotropy of Laser Powder Bed Fused Inconel 718</title>
    <abstract language="eng">Additive manufacturing methods such as laser powder bed fusion (LPBF) allow geometrically complex parts to be manufactured within a single step. However, as an aftereffect of the localized heat input, the rapid cooling rates are the origin of the large residual stress (RS) retained in as-manufactured parts. With a view on the microstructure, the rapid directional cooling leads to a cellular solidification mode which is accompanied by columnar grown grains possessing crystallographic texture. The solidification conditions can be controlled by the processing parameters and the scanning strategy. Thus, the process allows one to tailor the microstructure and the texture to the specific needs. Yet, such microstructures are not only the origin of the mechanical anisotropy but also pose metrological challenges for the diffraction-based RS determination. In that context the micromechanical elastic anisotropy plays an important role: it translates the measured microscopic strain to macroscopic stress. Therefore, it is of uttermost importance to understand the influence of the hierarchical microstructures and the texture on the elastic anisotropy of LPBF manufactured materials.&#13;
This study reveals the influence of the build orientation and the texture on the micro-mechanical anisotropy of as-built Inconel 718. Through variations of the build orientation and the scanning strategy, we manufactured specimens possessing [001]/[011]-, [001]-, and [011]/[111]-type textures. The resulting microstructures lead to differences in the macroscopic mechanical properties. Even further, tensile in-situ loading experiments during neutron diffraction measurements along the different texture components revealed differences in the microstrain response of multiple crystal lattice planes. In particular, the load partitioning and the residual strain accumulation among the [011]/[111] textured specimen displayed distinct differences measured up to a macroscopic strain of 10 %. However, the behavior of the specimens possessing [001]/[011]-and [001]-type texture was only minorly affected. The consequences on the metrology of RS analysis by diffraction-based methods are discussed.</abstract>
    <enrichment key="eventName">International Conference on Additive Manufacturing ICAM 2022</enrichment>
    <enrichment key="eventPlace">Orlando, FL, USA</enrichment>
    <enrichment key="eventStart">31.10.2022</enrichment>
    <enrichment key="eventEnd">04.11.2022</enrichment>
    <enrichment key="opus.source">publish</enrichment>
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    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <enrichment key="InvitedTalks">0</enrichment>
    <author>Jakob Schröder</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Laser powder bed fusion</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Neutron diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electron backscatter diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Mechanical behavior</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.6 Additive Fertigung metallischer Komponenten</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
  </doc>
  <doc>
    <id>56804</id>
    <completedYear/>
    <publishedYear>2022</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>lecture</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Fundamentals of diffraction-based residual stress and texture analysis of PBF-LB Inconel 718</title>
    <abstract language="eng">Laser powder bed fusion (PBF-LB/M) of metallic alloys is a layer wise additive manufacturing process which provides significant scope for more efficient designs of components, benefiting performance and weight, leading to efficiency improvements for various sectors of industry. However, to benefit from these design freedoms, knowledge of the high produced induced residual stress and mechanical property anisotropy associated with the unique microstructures is critical. X-ray and neutron diffraction are considered the benchmark for non-destructive characterization of surface and bulk internal residual stress. The latter, characterized by the high penetration power in most engineering alloys, allows for the use of diffraction angle close to 90° enabling a near cubic sampling volume to be specified. However, the complex microstructures of columnar growth with inherent crystallographic texture typically produced during PBF-LB/M of metallics present significant challenges to the assumptions typically required for time efficient determination of residual stress. These challenges include the selection of an appropriate set of diffraction elastic constants and a representative strain-free reference for the material of interest. In this presentation advancements in the field of diffraction-based residual stress analysis of L-PBF Inconel 718 will be presented. The choice of an appropriate set of diffraction-elastic constants depending on the underlying microstructure will be described.</abstract>
    <enrichment key="eventName">MLZ User Meeting 2022</enrichment>
    <enrichment key="eventPlace">Munich, Germany</enrichment>
    <enrichment key="eventStart">08.12.2022</enrichment>
    <enrichment key="eventEnd">09.12.2022</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="InvitedTalks">1</enrichment>
    <author>Jakob Schröder</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Residual Stress</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Microstructure</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Texture</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Mechanical behavior</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.6 Additive Fertigung metallischer Komponenten</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
  </doc>
  <doc>
    <id>63272</id>
    <completedYear/>
    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>1</pageFirst>
    <pageLast>9</pageLast>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>article</type>
    <publisherName>Wiley-VCH</publisherName>
    <publisherPlace>Weinheim</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>1</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">X-ray computed tomography quantifies primary phases and reveals crack morphology in high-cycle fatigue of aluminum alloy EN AW-2618A</title>
    <abstract language="eng">Since the introduction of high-strength aluminum alloys understanding their fatigue behavior is of high interest for the structural integrity of engineering components, in this context, the alloy EN AW-2618A gains its high strength from both nanometer size precipitates and micrometer size primary phases. The latter phases are often identified as crack initiation sites. In this study, it uses a combination of synchrotron and laboratory-based X-ray computed tomography to image and quantify such primary phases and the fatigue cracks appearing in interrupted tests. Based on the gray-level differences in the synchrotron X-ray computed tomography scans, this study is able to distinguish low- and high-absorbing particles. The dominant (volume fraction &gt;99%) high absorbing primary phase can be quantified in good agreement with results of Thermo-Calc calculations. To image the fatigue crack, laboratory X-ray computed tomography scans are performed at different tensile loads to open the crack. The results show that with an appropriate crack opening tensile load, the fatigue crack morphology can be reliably revealed. Based on these results, the influence of the primary phases on the fatigue crack initiation and propagation are discussed.</abstract>
    <parentTitle language="eng">Advanced engineering materials</parentTitle>
    <identifier type="doi">10.1002/adem.202500235</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-632724</identifier>
    <identifier type="issn">1527-2648</identifier>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="date_peer_review">17.06.2025</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Jakob Schröder</author>
    <author>Ying Han</author>
    <author>Tobias Fritsch</author>
    <author>Bardia Hejazi</author>
    <author>Alexander Ulbricht</author>
    <author>Birgit Skrotzki</author>
    <author>Giovanni Bruno</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>X-ray computed tomography</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Fatigue</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Aluminum</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Primary phases</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="institutes" number="">9.4 Integrität von Schweißverbindungen</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="themenfelder" number="">Degradationsmechanismen</collection>
    <collection role="literaturgattung" number="">Verlagsliteratur</collection>
    <collection role="fulltextaccess" number="">Datei für die Öffentlichkeit verfügbar ("Open Access")</collection>
    <collection role="unnumberedseries" number="">Wissenschaftliche Artikel der BAM</collection>
    <thesisPublisher>Bundesanstalt für Materialforschung und -prüfung (BAM)</thesisPublisher>
    <file>https://opus4.kobv.de/opus4-bam/files/63272/Adv Eng Mater_2025_Schroeder.pdf</file>
  </doc>
  <doc>
    <id>60294</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume/>
    <type>lecture</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>--</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Laser Powder Bed Fusion: Fundamentals of Diffraction-Based Residual Stress Determination</title>
    <abstract language="eng">The general term additive manufacturing (AM) encompasses processes that enable the production of parts in a single manufacturing step. Among these, laser powder bed fusion (PBF-LB) is one of the most commonly used to produce metal components. In essence, a laser locally melts powder particles in a powder bed layer-by-layer to incrementally build a part. As a result, this process offers immense manufacturing flexibility and superior geometric design capabilities compared to conventional processes. However, these advantages come at a cost: the localized processing inevitably induces large thermal gradients, resulting in the formation of large thermal stress during manufacturing. In the best case, residual stress remains in the final parts produced as a footprint of this thermal stress. Since residual stress is well known to exacerbate the structural integrity of components, their assessment is important in two respects. First, to optimize process parameter to minimize residual stress magnitudes. Second, to study their effect on the structural integrity of components (e.g., validation of numerical models). Therefore, a reliable experimental assessment of residual stress is an important factor for the successful application of PBF-LB. In this context, diffraction-based techniques allow the non-destructive characterization of the residual stress. In essence, lattice strain is calculated from interplanar distances by application of Braggs law. From the known lattice strain, macroscopic stress can be determined using Hooke’s law. To allow the accurate assessment of the residual stress distribution by such methods, a couple of challenges in regard of the characteristic PBF-LB microstructures need to be overcome. &#13;
This presentation highlights some of the challenges regarding the accurate assessment of residual stress in PBF-LB on the example of the Nickel-based alloy Inconel 718. The most significant influencing factors are the use of the correct diffraction elastic constants, the choice of the stress-free reference, and the consideration of the crystallographic texture. Further, it is shown that laboratory X-ray diffraction methods characterizing residual stress at the surface are biased by the inherent surface roughness. Overall, the impact of the characteristic microstructure is most significant for the selection of the correct diffraction elastic constants. In view of the localized melting and solidification, no significant gradients of the stress-free reference are observed, even though the cell-like solidification sub-structure is known to be heterogeneous on the micro-scale.</abstract>
    <enrichment key="eventName">4th Symposium on Materials and Additive Manufacturing</enrichment>
    <enrichment key="eventPlace">Berlin, Germany</enrichment>
    <enrichment key="eventStart">12.06.2024</enrichment>
    <enrichment key="eventEnd">14.06.2024</enrichment>
    <enrichment key="InvitedTalks">1</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">true</enrichment>
    <author>Jakob Schröder</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Additive Manufacturing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Residual Stress</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Electron Backscatter Diffraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Laser Powder Bed Fusion</value>
    </subject>
    <collection role="ddc" number="620">Ingenieurwissenschaften und zugeordnete Tätigkeiten</collection>
    <collection role="institutes" number="">5 Werkstofftechnik</collection>
    <collection role="institutes" number="">5.1 Mikrostruktur Design und Degradation</collection>
    <collection role="institutes" number="">5.2 Metallische Hochtemperaturwerkstoffe</collection>
    <collection role="institutes" number="">8 Zerstörungsfreie Prüfung</collection>
    <collection role="institutes" number="">8.5 Röntgenbildgebung</collection>
    <collection role="institutes" number="">9 Komponentensicherheit</collection>
    <collection role="themenfelder" number="">Material</collection>
    <collection role="fulltextaccess" number="">Datei im Netzwerk der BAM verfügbar ("Closed Access")</collection>
    <collection role="literaturgattung" number="">Präsentation</collection>
    <collection role="institutes" number="">9.6 Additive Fertigung metallischer Komponenten</collection>
    <collection role="themenfelder" number="">Additive Fertigung</collection>
  </doc>
</export-example>
