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    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue>10</issue>
    <volume>13</volume>
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    <title language="eng">Calorimetric and Dielectric Investigations of Epoxy-Based Nanocomposites with Halloysite Nanotubes as Nanofillers</title>
    <abstract language="eng">Epoxy nanocomposites are promising materials for industrial applications (i.e., aerospace, marine and automotive industry) due to their extraordinary mechanical and thermal properties. Here, the effect of hollow halloysite nanotubes (HNT) on an epoxy matrix (Ep) was the focus of the study. The structure and molecular mobility of the nanocomposites were investigated using a combination of X-ray scattering, calorimetry (differential (DSC) and fast scanning calorimetry (FSC)) and dielectric spectroscopy. Additionally, the effect of surface modification of HNT (polydopamine (PDA) and Fe(OH)3 nanodots) was considered. For Ep/HNT, the glass transition temperature (Tg) is was de-creased due to a nanoparticle-related decrease of the crosslinking density. For the modified system, Ep/m-HNT, the surface modification resulted in enhanced filler–matrix interactions leading to higher Tg values than the pure epoxy in some cases. For Ep/m-HNT, the amount of interface formed between the nanoparticles and the matrix ranged from 5% to 15%. Through BDS measurements, localized fluctuations were detected as a β- and γ-relaxation, related to rotational fluctuations of phenyl rings and local reorientations of unreacted components. A combination of calorimetry and BDS dielectric spectroscopy revealed a dynamic and structural heterogeneity of the matrix, as confirmed by two glassy dynamics in both systems, related to regions with different crosslinking densities.</abstract>
    <parentTitle language="eng">Polymers</parentTitle>
    <identifier type="doi">10.3390/polym13101634</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-526668</identifier>
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    <enrichment key="date_peer_review">03.06.2021</enrichment>
    <licence>Creative Commons - CC BY - Namensnennung 4.0 International</licence>
    <author>Hassan Omar</author>
    <author>Glen Jacob Smales</author>
    <author>S. Henning</author>
    <author>Z. Li</author>
    <author>D.-Y. Wang</author>
    <author>Andreas Schönhals</author>
    <author>Paulina Szymoniak</author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Rigid amorphous fraction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Epoxy nanocomposites</value>
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    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Halloysite nanotubes</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>X-ray scattering</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Differential scanning calorimetry</value>
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    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Broadband dielectric spectroscopy</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Flash DSC</value>
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    <collection role="institutes" number="">6 Materialchemie</collection>
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    <id>58250</id>
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    <publishedYear>2023</publishedYear>
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    <language>eng</language>
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    <edition/>
    <issue>11-12</issue>
    <volume>4</volume>
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    <title language="eng">Robocasting of ordered mesoporous silica‐based monoliths: Rheological, textural, and mechanical characterization</title>
    <abstract language="eng">Hierarchically porous, high‐surface‐area silica materials are excellent candidates for multiple applications like catalysis and environmental remediation. Shaping these materials with additive manufacturing (AM) techniques, like robocasting, could enable their use with the benefit of on‐demand, customized shaping and maximizing performance. Herein, ordered mesoporous silica COK‐12 slurries were robocasted into monoliths, containing different ratios of uncalcined COK‐12 and sodium bentonite (0–25 wt.%). The rheology of the mixed slurries is characterized by lower flow indexes (0.69 vs. 0.32) and higher yield stresses (96 vs. 259 Pa) compared to pure COK‐12 ones. Monoliths were printed in woodpile structures and calcined at 600°C. Micro‐CT measurements showed a linear shrinkage of 25% after calcination. Mechanical characterization showed increased uniaxial strength (0.20 ± 0.07 to 1.0 ± 0.3 MPa) with increasing binder/solids ratio from 13 to 25%. The amorphous, mesoporous structure of COK‐12 was retained. The structures exhibited open porosities of 52 ± 4% and showed higher specific mesopore volumes, and increased average mesopore size (6 vs. 8 nm) compared to COK‐12. Small‐angle x‐ray scattering analysis revealed an increased lattice parameter (10.3 vs. 11.0 nm) and reduced wall thickness (3.1 nm vs. 4.1 nm) of the COK‐12 in the monoliths. These properties indicate suitability for their application as porous supports and adsorbents.</abstract>
    <parentTitle language="eng">Nano Select</parentTitle>
    <identifier type="doi">10.1002/nano.202300109</identifier>
    <identifier type="urn">urn:nbn:de:kobv:b43-582503</identifier>
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Shaping these materials with additive manufacturing (AM) techniques, like robocasting, could enable their use with the benefit of on\u2010demand, customized shaping and maximizing performance. Herein, ordered mesoporous silica COK\u201012 slurries were robocasted into monoliths, containing different ratios of uncalcined COK\u201012 and sodium bentonite (0\u201325\u00a0wt.%). The rheology of the mixed slurries is characterized by lower flow indexes (0.69\u00a0vs. 0.32) and higher yield stresses (96\u00a0vs. 259\u00a0Pa) compared to pure COK\u201012 ones. Monoliths were printed in woodpile structures and calcined at 600\u00b0C. Micro\u2010CT measurements showed a linear shrinkage of 25% after calcination. Mechanical characterization showed increased uniaxial strength (0.20\u00a0\u00b1\u00a00.07 to 1.0\u00a0\u00b1\u00a00.3\u00a0MPa) with increasing binder\/solids ratio from 13 to 25%. The amorphous, mesoporous structure of COK\u201012 was retained. 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    <author>E. S. Dal Molin</author>
    <author>L. M. Henning</author>
    <author>J. T. Müller</author>
    <author>Glen Jacob Smales</author>
    <author>Brian Richard Pauw</author>
    <author>M. F. Bekheet</author>
    <author>A. Gurlo</author>
    <author>U. Simon</author>
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      <value>MOUSE</value>
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