Dokument-ID Dokumenttyp Autoren/innen Persönliche Herausgeber/innen Haupttitel Abstract Auflage Verlagsort Verlag Herausgeber (Institution) Erscheinungsjahr Titel des übergeordneten Werkes Jahrgang/Band ISBN Veranstaltung Veranstaltungsort Beginndatum der Veranstaltung Enddatum der Veranstaltung Ausgabe/Heft Erste Seite Letzte Seite URN DOI Lizenz Datum der Freischaltung OPUS4-53801 Zeitschriftenartikel Griesche, Axel; Pfretzschner, B.; Taparli, Ugur Alp; Kardjilov, N. Time-Resolved Neutron Bragg-Edge Imaging: A Case Study by Observing Martensitic Phase Formation in Low Temperature Transformation (LTT) Steel during GTAW Polychromatic and wavelength-selective neutron transmission radiography were applied during bead-on-plate welding on 5 mm thick sheets on the face side of martensitic low transformation temperature (LTT) steel plates using gas tungsten arc welding (GTAW). The in situ visualization of austenitization upon welding and subsequent α'-martensite formation during cooling could be achieved with a temporal resolution of 2 s for monochromatic imaging using a single neutron wavelength and of 0.5 s for polychromatic imaging using the full spectrum of the beam (white beam). The spatial resolution achieved in the experiments was approximately 200 µm. The transmitted monochromatic neutron beam intensity at a wavelength of λ = 0.395 nm was significantly reduced during cooling below the martensitic start temperature Ms since the emerging martensitic phase has a ~10% higher attenuation coefficient than the austenitic phase. Neutron imaging was significantly influenced by coherent neutron scattering caused by the thermal motion of the crystal lattice (Debye-Waller factor), resulting in a reduction in the neutron transmission by approx. 15% for monochromatic and by approx. 4% for polychromatic imaging. Basel MDPI 2021 Applied Sciences 11 22 10886 urn:nbn:de:kobv:b43-538016 10.3390/app112210886 https://creativecommons.org/licenses/by/4.0/deed.de 2021-11-22 OPUS4-57819 Zeitschriftenartikel Serrano Munoz, Itziar; Pfretzschner, Beate; Kromm, Arne; Nadammal, Naresh; Kardjilov, N.; Markötter, Henning; Neuwirth, T.; Schulz, M.; Griesche, Axel High-resolution Bragg-edge neutron radiography detects grain morphology in PBF-LB/M IN718 One of the main advantages of metal additive manufacturing (MAM) techniques is their ability to produce components with site-specific microstructural features. Nevertheless, microstructural defects and lack of repeatability are still major concerns in MAM. In this study, a laser powder bed fusion (PBF-LB/M) IN718 material, produced using two different scan length vectors, is investigated using Bragg-edge neutron 2D imaging (BENI) combined with electron backscatter diffraction (EBSD) analysis. BENI is able to detect, on a macroscopic scale, process-induced changes in texture in a large field of view covering the entire sample (20×80 mm2). In addition, high-resolution BENI (HR-BENI), with a pixel size of 12.8 µm, provides a micro-scale examination of the local variations of texture and grain morphology, otherwise undistinguishable using the standard resolution. As such, HR-BENI offers a straightforward and detailed way of screening the integrity of MAM parts at cm-length scales. Amsterdam Elsevier 2023 Materialia 30 1 6 10.1016/j.mtla.2023.101827 2023-07-03