TY  - CONF
A1  - Haferkamp, Sebastian
T1  - In situ monitoring of mechanochemical Knoevenagel condensations
N2  - Mechanaochemistry is an effective method to yield pure compounds within a short reaction time. Mechanochemical C-C bond forming reactions gained increasing interest in the past decade. Among those the Knoevenagel condensation is an important reaction for synthezing a,b-unsaturated compounds. The information on the underlying mechanisms of mechanochemical reactions are scarce. In situ investigations using Raman spectroscopy and synchroton XRD either alone or in combination address this challenge. We present the in situ results of a Knoevenagel condensation with p-nitrobenzaldehyde and malononitrile under neat grinding conditions.
T2  - Adlershofer Forschungsforum
CY  - Berlin, Germany
DA  - 10.11.2017
KW  - Mechanochemistry
KW  - Knoevenagel condensation
PY  - 2017
AN  - OPUS4-44140
LA  - eng
AD  - Bundesanstalt fuer Materialforschung und -pruefung (BAM), Berlin, Germany
ER  -