FG Füge- und Schweißtechnik
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3D-printed structured catalysts for CO2 methanation reaction: Advancing of gyroid-based geometries
(2022)
This work investigates the CO2 methanation rate of structured catalysts by tuning the geometry of 3D-printed metal Fluid Guiding Elements (FGEs) structures based on periodically variable pseudo-gyroid geometries. The enhanced performance showed by the structured catalytic systems is mostly associated with the capability of the
FGEs substrate geometries for efficient heat usages. Thus, variations on the channels diameter resulted in ca. 25% greater CO2 conversions values at intermediate temperature ranges. The highest void fraction evidenced in the best performing catalyst (3D-1) favored the radial heat transfer and resulted in significantly enhanced catalytic activity, achieving close to equilibrium (75%) conversions at 400 ◦C and 120 mL/min. For the 3D-1 catalyst, a mathematical model based on an experimental design was developed thus enabling the estimation of its behavior as a function of temperature, spatial velocity, hydrogen to carbon dioxide (H2/CO2) ratio, and inlet CO2 concentration.
Its optimal operating conditions were established under 3 different scenarios: 1) no restrictions, 2) minimum H2:CO2 ratios, and 3) minimum temperatures and H2/CO2 ratio. For instance, for the lattest scenario, the best CO2 methanation conditions require operating at 431 ◦C, 200 mL/min, H2/CO2 = 3 M ratio, and inlet CO2 concentration = 10 %.
This work presents the concept and testing of a new modification of a previously invented high-temperature resistant ultrasonic transducer for immersive thickness measurement. The modification lies in the removal of a front electrode and using the electrical conductivity of the surrounding liquid to transfer the electrical charge onto the liquid-contacted surface of a piezo actuator. By not using a front electrode the developed technology provides a considerable increase of the transducer sensitivity, as well as a significant improvement of the signal-to-noise ratio. Furthermore, it reduces the minimum measurable thickness by shortening the impulse due to minimization of the scattering of emitted signal caused by front electrode. Therefore, despite some isolated complications, which could arise in special cases of application of modified transducer, the presented concept provides an appreciable improvement of the measuring quality.
This work investigates heat transfer mechanism of aluminum resistance spot welding process. The main target is to determine thermal contact conductance and heat transfer coefficients for natural convection and thermal radiation at ambient air and forced convection inside the water-cooled electrodes. For this purpose, the heat transfer of hot sheets in a welding gun for aluminum alloys AA5182 and AA6014 is analyzed experimentally and numerically. The transient temperature field is measured by several thermocouples in a simplified experimental setup. Subsequent thermal-mechanical coupled finite
element simulations of the experiments were used to calibrate the heat transfer coefficients. The heat transfer coefficient for natural convection and thermal radiation to ambient air is 13 W m2 K and the heat transfer coefficient for forced convection of electrode water-cooling is 25,000 W m2 K. The results indicate that the thermal contact conductance can be assumed ideal for welding process. Additionally, the finite element model is validated by the measured and calculated dissipated heat due to forced convection. Finally, a sensitivity analysis is performed to compare the influence of maximum and minimum heat transfer coefficients of forced convection (water-cooling) on transient temperature field and dissipated heat of sample
AA5182.
For the reliability of many welded structures like pipelines or offshore wind parks, it is necessary to ensure high mechanical properties such as strength and toughness of the entire material. In order to improve quality of weld joints, flux cored rods and wires containing different nanoparticles (ZrO2, LaB6 and Al2O3) were manufactured and welded with the TIG and MAG welding processes. Influence of these nanoparticles on the microstructure and mechanical properties of the weld joints were investigated. The acicular ferrite and improved strength of the weld metals were observed by the addition of 0.2 wt.% of iron powder with ZrO2 nanoparticles to the filling of flux cored wires.
The properties of sandwiches with aluminum foam and the special features of their use in lightweight welded structures are determined. The weldability of such sandwiches in foamed and non-foamed conditions is analyzed under friction stir welding, laser beam welding and short arc welding in protective gas. The process and mechanical properties of the welds are studied. The results are generalized in a catalog that may be useful for materials scientists and designers.
Among different joining methods, the electron beam welding is recently applied for manufacturing of turbine components from temperature-resistant nickel-based conventionally cast Alloy 247 LC CC. However, the high tendency to hot cracking, in particular the formation of solidification cracks, remains a major challenge. Experiments indicate a significant reduction in hot cracks if the welding is performed outside the common welding parameter range. To understand these observations, a study of local thermo-mechanical conditions during electron beam welding of Alloy 247 samples was carried out using numerical simulations. The results were subsequently compared with reference test welds. For this purpose, a finite element model for coupled transient thermal and mechanical analysis was created and used. The work presents a comparative analysis of the evolution of strain components in brittle temperature range during cooling, considering the distribution and orientation of the cracks. Various relations between local strain kinetics and crack appearance, with notable influence of the plastic strain vector, were observed. Finally, the aspects of assessment of hot crack susceptibility with aid of thermo-mechanical welding simulation are discussed.
Analysis of temperature field during electron beam welding of hot crack sensitive nickel base alloy
(2021)
The use of temperature-resistant nickel-based superalloys in the field of industrial gas turbines is increasing due to constantly rising operating temperatures. Among different joining methods the electron beam welding is commonly used for manufacturing of turbine components because it provides a reduced heat input. However, the highly localized beam impact causes high temperature gradients and leads to the formation of hot cracks. Welding of such material with a high brittle temperature range is challenging and needs an increasing effort of process adaption. Experiments indicate a significant improvement of hot crack susceptibility when welding outside the common welding parameter range. To understand these observations a study of the temperature field in the specimens using numerical simulations was carried out. For this purpose, a validated simulation model was used. Special attention was paid to the domain in close vicinity of the weld pool. The results illustrate the velocity of solidification isotherm as well as the temperature rates when crossing the melting point. Finally, the relations between thermal fields, crack types and distributions in the different specimens are discussed.
Analytisches Schrumpfkraftmodell und Berechnungsprogramm zur Bestimmung des schweißbedingten Verzugs
(2008)
Anwendungsnahe Simulation des thermischen Richtens : Forschungsvorhaben P 1008/IGF-Nr. 17970 BR
(2016)
Application of macro-cellular SiC reactor to diesel engine-like injection and combustion conditions
(2012)
The microstructure and the distribution of chemical elements in laser-welded joints of Al – Mg – Si alloy 6005-T6 are studied. Segregations of chemical elements are detected over grain boundaries in the heat-affected zones of the welded joints. The joints fracture by the intergrain mechanism. A Gleeble 3800 device is used to determine the temperature dependences of the mechanical properties of the alloy with allowance for the special features of the welding cycle. Amethod for evaluating the sensitivity of welded joints of aluminum alloys to formation of liquation cracks with allowance for the local properties of the metal, the welding conditions, and the rigidity of the construction is suggested.
Der Vortrag stellt die Identifizierung und Bewertung der relevanten Einflussfaktoren auf die Gefügeumwandlungen und auf die thermomechanischen Werkstoffkennwerte bei komplexen Temperaturbelastungen vor. Dies erfolgt durch physikalische Simulation der Gefüge in der WEZ von Mehrlagenschweißungen und Aufnahme von Dilatometerkurven und Spannungs-Dehnungskurven. Es wurden einflussarme Kombination von Temperaturzyklen und weitere mit starkem Einfluss auf die Gefügeumwandlung identifiziert. Hinweise zu den erforderlichen Werkstoffkennwerten für die numerische Schweißsimulation wurden gegeben.
Calculation of thermal processes in welding thick plates with moving axisymmetric heat sources
(2016)
Due to recent developments, cold gas spraying technology can now be used to create inner diameter coatings for cylinder inner diameters > 70 mm. The present investigations focus on the process optimization and the specific properties of cold gas spray inner diameter coatings created with three different alloy steel powder variants. The cold gas spray coating properties were compared with the corresponding properties of coatings created with twin wire arc technology. The particle velocities and deposition efficiencies were measured with the aim of optimizing the process parameters. The most suitable process parameters were used to analyze the microstructure of the deposited coating in terms of porosity and interface quality. Furthermore, the hardness and adhesion strength properties of the coatings were measured. In addition, the different liners were honed, and the achievable surface roughness of each was determined. Finally, wear resistance was evaluated using ball-on-disk testing. The results reveal that with the maximum process parameters, the cold gas spray coating properties are comparable to the twin wire arc coating properties. Further investigations are necessary to determine whether cold gas spraying is a feasible alternative to the current series production process for cylinder surface coatings.
The properties of the welded joints of 6082-T6 alloy produced by friction stir welding (FSW) and laser welding(LW) were studied. The maximum temperature and microhardness fields in the friction stir-welded joints were shown to be asymmetrical. The concentrated energy input during laser welding yields a narrow heat-affected zone (HAZ) with sharp changes in mechanical properties. The strength of the FSW joint constitutes 72% and that of the LWjoint—67% of the base metal strength. In case of LW, the minimum hardness of the joint corresponds to the metal of the welded joint, while in case of FSW, it corresponds to the heat-affected zone. At the same maximum heating temperature, the hardness of the heat-affected zone of the friction stir-welded joint is lower compared to laser welding due to substantially lower rates of heating and cooling.
The purpose of this study is to characterise the corrosion behaviour of zinc-coated sheet metals after a structuring process using the salt spray test. The investigated structured material is manufactured by hydroforming and has a periodic hexagonal geometry. The corrosion behaviour has been evaluated by estimating the development of the corrosion area and penetration depth. The results of the investigation show that the corrosion area is larger on the smooth sheet than on the structured sheet. The difference between the structured and smooth sheets is negligible with increasing exposure time. Furthermore, the reasons for the different corrosion behaviours are discussed.
Crystallography and Mechanical Properties of Wire Arc Additively Manufactured Al5356 Components
(2021)
In this study, we present results of the evolution of the crystallographic texture and imperfections, as well as the corresponding mechanical properties of wire and arc additively manufactured (WAAM) Al5356 specimens, studied by X-ray diffraction (XRD) and tensile testing, respectively. The results show that the phase composition is in the form of a face-centred cubic (fcc) crystal structure, corresponding to the base material, as well as some traces of oxide phase Al2O3. The WAAM specimen growing is accompanied by a slight change in the preferred crystallographic orientation, from (111) to (200) and a decrease in the imperfections concentration. Also, it was found that the ultimate tensile strength (UTS), yield strength (YS), and elongation slightly decrease from the initial to the more advanced stages of growth.
Direct bonding of copper and porous LaCrO₃ without an extra filler interlayer was successfully completed using local and fast Cu‐infiltration through laser cladding. This significantly reduced the susceptibility of the ceramic to cracking. A high‐speed camera investigation into the wetting and infiltration behavior of a Cu‐melt into LaCrO₃ with a porosity of ~63 vol% was performed. By adjusting the focal distance with a constant laser power of 300 W, the Cu‐melt was rapidly infiltrated into the ceramic preform in 10 seconds. This was completed under atmospheric air conditions, without added inert gas. The joining process developed can be used to fabricate ceramic/metal joints with targeted (micro‐) structure properties by adjusting the infiltrated melt and the infiltration depth, which would be suitable for many applications, such as multifunctional devices, solid oxide fuel cells or heating elements.
Deposition of Ti-6Al-4V using laser and wire, part II: Hardness and dimensions of single beads
(2011)
This study presents an experimental results of residual stress states in stainless steel plate samples with size 100 x 50 x 10 mm welded using a high-power fiber laser. The technological parameters of the welding process were: laser power Q = 15 kW; laser spot size = 0.65 mm; welding speed V = 3 m/min; 4 m/min; 5 m/min, using 30 L/min of protective Ar gas. The neutron diffraction method was used to determine the residual stresses in the bulk of the material. The neutron experiments were performed on the FSD diffractometer at the IBR-2 pulsed reactor in the Frank Laboratory of Neutron Physics, Joint Institute for Nuclear Research - Dubna, Russian Federation. The measured residual stress distributions exhibit maxima at weld seam centers. As expected, for all specimens the residual stress is falling down in regions distant from the weld zone. Maximal residual stress value of 492 MPa was observed for sample welded with speed of V = 5 m/min.
The work deals with the elastic-plastic thermo-mechanical deformation process after spot heating of large thin plates. It promotes a new theoretical model of the process. The main target is to clarify the kinetics of the plastic strain formation during thermal straightening and to explore the main interactions. For this purpose, a simplified mechanical problem is formulated and applied. As a result, definite thermo-mechanical relations between temperature, initial strain, and accumulated plastic strain are obtained. Finally, a verification study is presented and discussed. The results contribute to extending the knowledge about the process and to establishing a theoretical background for development of applied analytical or analytical-numerical approaches for practical use in the designing and planning phases in welding production. An application to a particular case is described in an accompanying paper (part 2).
An analytical model based on a theoretical model established in the previous work (part 1) is developed. The analytical model considers the particular case of an instantaneous high-density heat source acting on a thin pre-stressed plate. It calculates the plastic strain and the area of the zone of plastic deformation. A theoretical study is performed in order to quantify the major factors that influence the plastic strain formation. Furthermore, the work presents a calculation procedure for distortion analysis of lar ge and complex structures, intended to be used for solving industrial tasks. The calculation procedure consists of a combination of the analytical solution and an elastic finite element analysis with the aid of the inherent strain approach. Various aspects of its application are also discussed. The calculation procedure is finally explained using a simple example. Its reliability and practicability are demonstrated through verification and validation studies. The work is dedicated to the thermal straightening of thin-walled welded structures; however, it can also be related to other processes.
The work presents an innovative approach for simulation of welding induced distortions, which allows taking into consideration the local effects of the welding process as well as the global interactions in the structure. The approach bases on an integration of analytical and numerical calculation’s procedures in a hybrid model, realized with the aid of the inherent strain concept. The analytical procedure calculates the shrinkage strain components and area of the plastic deformed zone, caused by welding. The calculated strains are then transferred to the global finite element model in order to predict the distortions and stresses in the structure after every welding stage, as well as their final state. The consideration of welding scenarios, weld sequence, clamping conditions and the assembling stages is done by taking into account the intermediate variation of the strain state during the manufacturing steps.
The article gives the theoretical basis of the analytical model. The consideration of the essential physical relations is put into discussion. The application of the model is illustrated on complex structures. Its reliability and practicability are demonstrated by means of a validation study.
The formation of acicular ferrite in the structure of weld deposits when welding carbon steels is often associated with the introduction of nonmetallic additives into the electrode material. Fe–alumina composite powders with alumina particles less than 1 µm were used as a filler for cored welding wire and the influence of aluminum oxide additives up to 2,5 wt.% on the structure of the welded seam was studied. It was shown that the addition of aluminum oxide to the welding wire led to the initiation of the formation of intragranular acicular ferrite in the weld deposit and to a more even distribution of hardness through the zones of weld seam.
Amethod for assessing the effect of the temperature of friction stir welding on the microstructure and mechanical properties of welded joints of aluminum alloy D16AT is suggested. The temperature cycles in different zones of a welded joint are determined by mathematical simulation. The computed temperature cycles are implemented in a Gleeble-3800 system. It is shown that the welding temperature affects little the evolution of the microstructure in different zones of the welded joints of alloy D16AT.