FG Füge- und Schweißtechnik
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Institute
This work presents a comparative study towards the development of efficient micro-reactors based on 3D-printed structures. Thus, the study evaluates the influence of the metal substrate geometry on the performance of structured catalysts for the CO2 methanation reaction. For this purpose, 0.5%Ru–15%Ni/MgAl2O4 catalyst is wash coated over two different micro-monolithic metal substrates: a conventional parallel channel honeycomb structure and a novel 3D-printed structure with a complex gyroid geometry. The effect of the metal substrate geometry is analyzed for several CO2 sources including ideal flue gas atmospheres, the presence of residual CH4 and CO in the flue gas, as well as simulated biogas sources. The advantages of the gyroid-3D complex geometries over the honeycomb structures are shown for all evaluated conditions, providing at the best-case scenario a 14% improvement of CO2 conversion. Moreover, this contribution shows that systematically tailoring geometrical features of structured catalysts becomes an effective strategy to achieve improved catalysts performances independent of the flue gas composition. By enhancing the transport processes and the gas-catalyst interactions, the employed gyroid 3D metal substrates enable boosted CO2 conversions and greater CH4 selectivity within diffusional controlled regimes.
Deposition of Ti-6Al-4V using laser and wire, part II: Hardness and dimensions of single beads
(2011)
The formation of acicular ferrite in the structure of weld deposits when welding carbon steels is often associated with the introduction of nonmetallic additives into the electrode material. Fe–alumina composite powders with alumina particles less than 1 µm were used as a filler for cored welding wire and the influence of aluminum oxide additives up to 2,5 wt.% on the structure of the welded seam was studied. It was shown that the addition of aluminum oxide to the welding wire led to the initiation of the formation of intragranular acicular ferrite in the weld deposit and to a more even distribution of hardness through the zones of weld seam.
Numerical models for thermo-mechanical simulation of the welding
residual stresses in laser beam and multi-pass arc welded joints are developed. The models describe the resulting microstructure as a function of the peak temperature, austenization time, cooling time and take into account the microstructure formed after
single or multiple thermal cycles. The results of simulations are validated by neutron diffraction experiments performed on FSD diffractometer at the IBR-2 pulsed reactor in FLNP JINR (Dubna, Russia). The elaborated numerical models are in good agreement
with obtained neutron diffraction data, which enable to study the influence of different conditions and process parameters on the distribution of residual welding stresses.
Cored wires are used in numerous welding processes with or without extern al gas or flux shielding. Submerged are welding (SAW) with eored wires, seamed or seamless, for joining mild and low alloyed steel grades is a technique that has demonstrated clear advantages during the three last decades. Ever since its invention, the SAW process has evolved with one main goal: to combine quality with produetivity. With low alloy wires, the benefits have already been clearly demonstrated and widely exploited. However, little has been written on SA Wand cladding with eored wires for eorrosion or he at resisting applieations. Its extension to high alloy eompositions brings eorresponding benefits and adds so me specific and unique features. This paper foeuses on consumable specificities and on the quality and productivity features of SAW with CRA (corrosion resistant alloy) cored wires. It deseribes the potential as weIl as the limitations ofthis technique. Cored wires are now used for submerged are welding of almost aIl stainless steels ranging from soft martensitic to super-duplex, and for aseries of nickel base compositions as weIl as for cladding cobalt base aIloys. Examples of industrial applications with austenitic, duplex, martensitic and heat resisting stainless steels are given to illustrate the potential ofthe eored wire solution.