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  <doc>
    <id>27619</id>
    <completedYear/>
    <publishedYear>2021</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber>11</pageNumber>
    <edition/>
    <issue/>
    <volume>22</volume>
    <type>articler</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>2021-07-12</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Gold surface cleaning by etching polishing: Optimization of polycrystalline film topography and surface functionality for biosensing</title>
    <abstract language="eng">Modern bio-chemical sensors rely on functional interfacial architectures with well-defined structural nano-motifs over a physical transducer. Gold-coated interfaces are of particular interest for their desirable chemical (functionalization) and optical (plasmonic) properties. Here we investigate the cleaning and polishing of polycrystalline gold films in preparation of advanced surface functionalization. We focus on soft wet chemical etching to decrease the small-scale roughness commonly observed after evaporation or sputtering of gold. We show that optimized surfaces are obtained by etching in solutions of hydrochloric acid and hydrogen peroxide. We systematically quantify the films wettability, surface nano-topography, UV-VIS spectrum and the electrochemical and Surface Plasmon Resonance (SPR) changes throughout the etching process. Optimal results are obtained by etching with a HCl(37%):H2O2(30%):H2O mixture, with a volume ratio of reagents 3:3:94 during 15-20 minutes at room temperature for the main step. This reduces by a factor two the root-mean-square roughness, removes contaminants, increases hydrophilicity and modifies the gold surface by Au(Cl)x complexes. Significantly, the resulting the surface is hydrophilic enough to prevent globular proteins such as HSA to unfold upon deposition at concentrations more than ~1 mg/mL. Our protocol offers a simple, reliable and rapid method for the preparation of gold surface in view of further functionalization including the binding of receptor layers and various micro- and nanostructures required in chemical and biochemical sensing.</abstract>
    <parentTitle language="eng">Surfaces and Interfaces</parentTitle>
    <identifier type="doi">10.1016/j.surfin.2020.100818</identifier>
    <identifier type="issn">2468-0230</identifier>
    <enrichment key="BTU">an der BTU erstellt / created at BTU</enrichment>
    <enrichment key="Artikelnummer">100818</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="Fprofil">2 Gesundheit und Lifes Sciences / Health and Life Sciences</enrichment>
    <enrichment key="Fprofil">4 Künstliche Intelligenz und Sensorik / Artificial Intelligence and Sensor Technology</enrichment>
    <author>
      <firstName>Borys A.</firstName>
      <lastName>Snopok</lastName>
    </author>
    <submitter>
      <firstName>Karin</firstName>
      <lastName>Tonder</lastName>
    </submitter>
    <author>
      <firstName>Arwa</firstName>
      <lastName>Laroussi</lastName>
    </author>
    <author>
      <firstName>Clodomiro</firstName>
      <lastName>Cafolla</lastName>
    </author>
    <author>
      <firstName>Kislon</firstName>
      <lastName>Voitchovsky</lastName>
    </author>
    <author>
      <firstName>Tetiana V.</firstName>
      <lastName>Snopok</lastName>
    </author>
    <author>
      <firstName>Vladimir M.</firstName>
      <lastName>Mirsky</lastName>
    </author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>polycrystalline gold films</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>soft wet chemical polishing</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>gold cleaning</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>hydrochloric acid and hydrogen peroxide</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>protein adsorption</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>surface plasmon resonance</value>
    </subject>
    <collection role="institutes" number="2108">FG Nanobiotechnologie</collection>
  </doc>
  <doc>
    <id>34486</id>
    <completedYear/>
    <publishedYear>2024</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>3865</pageFirst>
    <pageLast>3877</pageLast>
    <pageNumber>13</pageNumber>
    <edition/>
    <issue>15</issue>
    <volume>6</volume>
    <type>articler</type>
    <publisherName>Royal Society of Chemistry (RSC)</publisherName>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>2024-11-11</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Agglomeration compaction promotes corrosion of gold nanoparticles</title>
    <abstract language="eng">Engineered nanoparticles are increasingly being used in various areas of human activity. However, the degradation mechanism of nanobodies in harsh environments is still a puzzle for theory and experiment. We report here the results of optical spectroscopy and nanoparticle tracking analysis, quantifying agglomeration and sizing of 50 nm citrate stabilized gold nanoparticles (GNPs) in HCl solutions containing H2O2. The mechanism of a consecutive corrosion reaction of GNPs is discussed within the framework of the near-field approach. We found that the disappearance of single nanoparticles from a suspension does not occur due to their dissolution per se, but is a consequence of the formation of aggregates. The neutralization of electrostatic shielding at high ionic strength allows gold nanoparticles to approach the subnanometer distance within the region of capping defects, at which the Casimir and van der Waals attractive forces dominate. It is suggested that electric field fluctuations in the confined space between highly conductive gold nanoparticles cause complexant-stimulated loss of metal from the core in the contact area. Going beyond the charge screening limitations by constraining the reaction space and reducing the double electrical layer thickness allows for chemical processes flow along otherwise not accessible reaction pathways.</abstract>
    <parentTitle language="eng">Nanoscale Advances</parentTitle>
    <identifier type="doi">10.1039/D4NA00109E</identifier>
    <identifier type="issn">2516-0230</identifier>
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Nauki, Kyiv, 03028, Ukraine"}]},{"ORCID":"http:\/\/orcid.org\/0000-0002-8427-4206","authenticated-orcid":false,"given":"Vladimir M.","family":"Mirsky","sequence":"additional","affiliation":[{"name":"Nanobiotechnology \u2013 Institute of Biotechnology, Brandenburg Technical University, Cottbus-Senftenberg, Universit\u00e4tsplatz 1, Senftenberg, 01968, Germany"}]}],"member":"292","published-online":{"date-parts":[[2024]]},"reference":[{"key":"D4NA00109E\/cit1\/1","doi-asserted-by":"crossref","first-page":"43","DOI":"10.1007\/s11051-023-05690-w","volume":"25","author":"Abbasi","year":"2023","journal-title":"J. Nanopart. Res."},{"issue":"2","key":"D4NA00109E\/cit2\/1","doi-asserted-by":"crossref","first-page":"415","DOI":"10.1016\/j.jcis.2006.07.059","volume":"303","author":"Li","year":"2006","journal-title":"J. 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