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  <doc>
    <id>27169</id>
    <completedYear/>
    <publishedYear>2021</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume>2021</volume>
    <type>image</type>
    <publisherName>Deutsche Physikalische Gesellschaft e.V.</publisherName>
    <publisherPlace>Bad Honnef</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>2021-03-16</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">High temperature reduction and reoxidation of cerium oxide on Cu(111)</title>
    <abstract language="eng">Cerium oxide is of great interest due to its technological importance in various electronic, optical and catalytic applications. The inverse model catalyst cerium oxide on Cu(111) shows a high activity for the production of methanol. Oxygen vacancies, e.g. in form of reduced ceria, are necessary for the production of methanol from CO2 and H2. The reduction of ceria may be achieved by exposure to H2 at elevated temperatures. We studied the interaction of H2 and CO2 with cerium oxide islands on a Cu(111) substrate with low-energy electron microscopy (LEEM) and x-ray absorption spectroscopy (XAS). From earlier studies, the orientation of the cerium oxide is known to be decisive for the catalytic activity. In our experiments, the impact of both orientations are directly compared via growth of (100) and (111) cerium oxide islands side by side. At temperatures around 550 °C, exposure to H2 leads to partial reduction and exposure to CO2 leads to complete reoxidation of the cerium oxide. The (100) and (111) orientations show different reduction and reoxidation behaviors.</abstract>
    <parentTitle language="eng">Verhandlungen der DPG - SurfaceScience21</parentTitle>
    <identifier type="url">https://www.dpg-verhandlungen.de/year/2021/conference/surfacescience/part/o/session/74/contribution/7</identifier>
    <enrichment key="BTU">an der BTU erstellt / created at BTU</enrichment>
    <enrichment key="Artikelnummer">O 74.7</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">false</enrichment>
    <enrichment key="Fprofil">1 Energiewende und Dekarbonisierung / Energy Transition and Decarbonisation</enrichment>
    <enrichment key="Fprofil">4 Künstliche Intelligenz und Sensorik / Artificial Intelligence and Sensor Technology</enrichment>
    <author>
      <firstName>Linus</firstName>
      <lastName>Pleines</lastName>
    </author>
    <submitter>
      <firstName>Karsten</firstName>
      <lastName>Henkel</lastName>
    </submitter>
    <author>
      <firstName>Lars</firstName>
      <lastName>Buß</lastName>
    </author>
    <author>
      <firstName>Tevfik Onur</firstName>
      <lastName>Menteş</lastName>
    </author>
    <author>
      <firstName>Francesca</firstName>
      <lastName>Genuzio</lastName>
    </author>
    <author>
      <firstName>Andrea</firstName>
      <lastName>Locatelli</lastName>
    </author>
    <author>
      <firstName>Jan Ingo</firstName>
      <lastName>Flege</lastName>
    </author>
    <author>
      <firstName>Jens</firstName>
      <lastName>Falta</lastName>
    </author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Cerium oxide</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>H2 interaction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>CO2 interaction</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Low-energy electron microscopy (LEEM)</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>X-ray absorption spectroscopy (XAS)</value>
    </subject>
    <collection role="institutes" number="1503">FG Angewandte Physik und Halbleiterspektroskopie</collection>
  </doc>
  <doc>
    <id>30499</id>
    <completedYear/>
    <publishedYear>2023</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst/>
    <pageLast/>
    <pageNumber/>
    <edition/>
    <issue/>
    <volume>732</volume>
    <type>articler</type>
    <publisherName/>
    <publisherPlace/>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>2023-03-21</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Cleaning and tailoring the Pt3Sn(111) surface for surface experiments</title>
    <abstract language="eng">The cleaning process of the bimetallic Pt3Sn(111) surface has been studied by means of low-energy electron microscopy (LEEM), microspot low-energy electron diffraction (-LEED), and X-ray photoemission electron microscopy (XPEEM). Different cleaning procedures, performed under ultra-high vacuum conditions (UHV), including sputtering with argon ions and repeated cycles of annealing up to 1500 K were investigated. In this work, we show that a clean Pt3Sn(111) surface of high structural quality with a sharp and brilliant (2 × 2) bulk reconstruction in LEED as well as a perfectly smooth surface with terraces of micron size can be achieved by sputtering, annealing at very high temperatures, followed by a subsequent slow (0.09 K/s) and careful cooling procedure. Additionally, we show the possibility of tailoring the Sn concentration in the topmost layers of Pt3Sn(111) as a function of annealing temperature and subsequent cooling rate. Structural changes of the surface are induced by Sn segregation combined with a surface order–disorder transition at 1340 K. Moreover, two new surface reconstructions depending on the cooling rate are reported.</abstract>
    <parentTitle language="eng">Surface Science</parentTitle>
    <identifier type="issn">0039-6028</identifier>
    <identifier type="issn">1879-2758</identifier>
    <identifier type="doi">10.1016/j.susc.2023.122281</identifier>
    <enrichment key="BTU">an der BTU erstellt / created at BTU</enrichment>
    <enrichment key="Artikelnummer">122281</enrichment>
    <enrichment key="opus.source">publish</enrichment>
    <enrichment key="opus.doi.autoCreate">false</enrichment>
    <enrichment key="opus.urn.autoCreate">false</enrichment>
    <enrichment key="Fprofil">1 Energiewende und Dekarbonisierung / Energy Transition and Decarbonisation</enrichment>
    <enrichment key="Fprofil">4 Künstliche Intelligenz und Sensorik / Artificial Intelligence and Sensor Technology</enrichment>
    <author>
      <firstName>Nicolas</firstName>
      <lastName>Braud</lastName>
    </author>
    <submitter>
      <firstName>Karsten</firstName>
      <lastName>Henkel</lastName>
    </submitter>
    <author>
      <firstName>Lars</firstName>
      <lastName>Buß</lastName>
    </author>
    <author>
      <firstName>Edvin</firstName>
      <lastName>Lundgren</lastName>
    </author>
    <author>
      <firstName>Lindsay R.</firstName>
      <lastName>Merte</lastName>
    </author>
    <author>
      <firstName>Harald J.</firstName>
      <lastName>Wallander</lastName>
    </author>
    <author>
      <firstName>Jon-Olaf</firstName>
      <lastName>Krisponeit</lastName>
    </author>
    <author>
      <firstName>Andrea</firstName>
      <lastName>Locatelli</lastName>
    </author>
    <author>
      <firstName>Tevfik Onur</firstName>
      <lastName>Mentes</lastName>
    </author>
    <author>
      <firstName>Matteo</firstName>
      <lastName>Jugovac</lastName>
    </author>
    <author>
      <firstName>Jan Ingo</firstName>
      <lastName>Flege</lastName>
    </author>
    <author>
      <firstName>Jens</firstName>
      <lastName>Falta</lastName>
    </author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Pt3Sn</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Low-energy electron microscopy (LEEM)</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Platinum</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Tin</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Cleaning</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Alloy</value>
    </subject>
    <collection role="institutes" number="1503">FG Angewandte Physik und Halbleiterspektroskopie</collection>
  </doc>
  <doc>
    <id>35933</id>
    <completedYear/>
    <publishedYear>2025</publishedYear>
    <thesisYearAccepted/>
    <language>eng</language>
    <pageFirst>12465</pageFirst>
    <pageLast>12472</pageLast>
    <pageNumber>8</pageNumber>
    <edition/>
    <issue>19</issue>
    <volume>17</volume>
    <type>articler</type>
    <publisherName>Royal Society of Chemistry (RSC)</publisherName>
    <publisherPlace>London</publisherPlace>
    <creatingCorporation/>
    <contributingCorporation/>
    <belongsToBibliography>0</belongsToBibliography>
    <completedDate>2025-05-16</completedDate>
    <publishedDate>--</publishedDate>
    <thesisDateAccepted>--</thesisDateAccepted>
    <title language="eng">Rubidium intercalation in epitaxial monolayer graphene</title>
    <abstract language="eng">Alkali metal intercalation of graphene layers has been of particular interest due to potential applications in electronics, energy storage, and catalysis. Rubidium (Rb) is one of the largest alkali metals and among the least investigated as an intercalant. Here, we report a systematic investigation, with a multi-technique approach, of the phase formation of Rb under epitaxial monolayer graphene on SiC(0001). We explore a wide phase space with two control parameters: the Rb density (i.e., deposition time) and sample temperature (i.e., room and low temperature). We reveal the emergence of (2 × 2) and [sqrt(3) x (sqrt3)] R30° structures formed by a single alkali metal layer intercalated between monolayer graphene and the interfacial C-rich reconstructed surface, also known as the buffer layer. Rb intercalation also results in strong n-type doping of the graphene layer. Upon progressively annealing to higher temperatures, we first reveal the diffusion of Rb atoms, which results in the enlargement of intercalated areas. As desorption sets in, intercalated regions progressively shrink and fragment. Eventually, at approximately 600 °C, the initial surface is retrieved, indicating the reversibility of the intercalation process.</abstract>
    <parentTitle language="eng">Nanoscale</parentTitle>
    <identifier type="doi">10.1039/D5NR00417A</identifier>
    <identifier type="issn">2040-3364</identifier>
    <enrichment key="Fprofil">1 Energiewende und Dekarbonisierung / Energy Transition and Decarbonisation</enrichment>
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Silvestro 12, 56127 Pisa, Italy"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2171-7081","authenticated-orcid":false,"given":"Stefano","family":"Veronesi","sequence":"additional","affiliation":[{"name":"NEST, Istituto Nanoscienze-CNR and Scuola Normale Superiore, Piazza S. Silvestro 12, 56127 Pisa, Italy"}]},{"given":"Tevfik Onur","family":"Mentes","sequence":"additional","affiliation":[{"name":"Applied Physics and Semiconductor Spectroscopy, Brandenburg University of Technology Cottbus-Senftenberg, 03046, Cottbus, Germany"}]},{"given":"Lars","family":"Bu\u00df","sequence":"additional","affiliation":[{"name":"Elettra-Sincrotrone Trieste S.C.p.A., Strada Statale 14, km 163.5, I-34149 Basovizza, Trieste, Italy"}]},{"given":"Antonio","family":"Rossi","sequence":"additional","affiliation":[{"name":"Center for Nanotechnology Innovation@NEST, Istituto Italiano di Tecnologia, Piazza S. 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    <title language="eng">High-temperature growth of CeOx on Au(111) and behavior under reducing and oxidizing conditions</title>
    <abstract language="eng">Inverse oxide–metal model catalysts can show superior activity and selectivity compared with the traditional supported metal–oxide architecture, commonly attributed to the synergistic overlayer–support interaction. We have investigated the growth and redox properties of ceria nanoislands grown on Au(111) between 700 and 890 °C, which yields the CeO2–Au(111) model catalyst system. We have observed a distinct correlation between deposition temperature, structural order, and oxide composition through low-energy electron microscopy, low-energy electron diffraction, intensity–voltage curves, and X-ray absorption spectroscopy. Improved structural order and thermal stability of the oxide have been achieved by increasing the oxygen chemical potential at the substrate surface using reactive oxygen (O/O2) instead of molecular O2 during growth. In situ characterization under reducing (H2) and oxidizing atmospheres (O2, CO2) indicates an irreversible loss of structural order and redox activity at high reduction temperatures, while moderate temperatures result in partial decomposition of the ceria nanoislands (Ce3+/Ce4+) to metallic cerium (Ce0). The weak interaction between Au(111) and CeOx would facilitate its reduction to the Ce0 metallic state, especially considering the comparatively strong interaction between Ce0 and Au0. Besides, the higher reactivity of atomic oxygen promotes a stronger interaction between the gold and oxide islands during the nucleation process, explaining the improved stability. Thus, we propose that by driving the nucleation and growth of the ceria/Au system in a highly oxidizing regime, novel chemical properties can be obtained.</abstract>
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    <author>
      <firstName>Lars</firstName>
      <lastName>Buß</lastName>
    </author>
    <author>
      <firstName>Emilia</firstName>
      <lastName>Pożarowska</lastName>
    </author>
    <author>
      <firstName>Carlos</firstName>
      <lastName>Morales</lastName>
    </author>
    <author>
      <firstName>Sanjaya D.</firstName>
      <lastName>Senanayake</lastName>
    </author>
    <author>
      <firstName>Mauricio J.</firstName>
      <lastName>Prieto</lastName>
    </author>
    <author>
      <firstName>Liviu C.</firstName>
      <lastName>Tănase</lastName>
    </author>
    <author>
      <firstName>Lucas</firstName>
      <lastName>de Souza Caldas</lastName>
    </author>
    <author>
      <firstName>Aarti</firstName>
      <lastName>Tiwari</lastName>
    </author>
    <author>
      <firstName>Thomas</firstName>
      <lastName>Schmidt</lastName>
    </author>
    <author>
      <firstName>Miguel A.</firstName>
      <lastName>Niño</lastName>
    </author>
    <author>
      <firstName>Michael</firstName>
      <lastName>Foerster</lastName>
    </author>
    <author>
      <firstName>Jens</firstName>
      <lastName>Falta</lastName>
    </author>
    <author>
      <firstName>Jan Ingo</firstName>
      <lastName>Flege</lastName>
    </author>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Inverse oxide-metal model catalysts</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Ceria nanoislands</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Growth</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Redox properties</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Low-energy electron microscopy (LEEM)</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Low-energy electron diffraction (LEED)</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>Intensity–voltage curves</value>
    </subject>
    <subject>
      <language>eng</language>
      <type>uncontrolled</type>
      <value>X-ray absorption spectroscopy (XAS)</value>
    </subject>
    <collection role="institutes" number="1503">FG Angewandte Physik und Halbleiterspektroskopie</collection>
  </doc>
</export-example>
