@misc{MiahKloshekGonzalezCastanoetal., author = {Miah, Kamal Uddin Mohammad and Kloshek, Alexander and Gonz{\´a}lez-Casta{\~n}o, Miriam and Kehm, Christian and Ossenbrink, Ralf and Michailov, Vesselin}, title = {Herstellen hocheffektiver Mikroreaktoren durch selektives Laserstrahlschmelzen}, series = {DVS Congress 2022, Große Schweißtechnische Tagung, DVS Campus ; Kurzfassungen der Vortr{\"a}ge der Veranstaltung in Koblenz vom 19. bis 21. September 2022 ; (Langfassungen der Beitr{\"a}ge auf USB-Karte)}, journal = {DVS Congress 2022, Große Schweißtechnische Tagung, DVS Campus ; Kurzfassungen der Vortr{\"a}ge der Veranstaltung in Koblenz vom 19. bis 21. September 2022 ; (Langfassungen der Beitr{\"a}ge auf USB-Karte)}, publisher = {DVS Media GmbH}, address = {D{\"u}sseldorf}, isbn = {978-3-96144-189-1}, pages = {708 -- 713}, abstract = {Das pulverbasierte 3D-Metalldrucken erm{\"o}glicht die Fertigung von hochkomplexen Integralbauteilen, die als Tr{\"a}gerstruktur f{\"u}r Mikroreaktoren benutzt werden. Nach einer Beschichtung der Struktur mit einem Katalysatormaterial, k{\"o}nnen diese Mikroreaktoren h{\"o}chst effizient f{\"u}r die CO2-Methanisierung eingesetzt werden. Durch die additive Fertigung mit dem selektiven Laserstrahlschmelzen (SLM) wurden adaptierte dreidimensionale periodische Gitterstrukturen mit sehr geringen Wandst{\"a}rken hergestellt. Diese weisen ein sehr g{\"u}nstiges Verh{\"a}ltnis von Oberfl{\"a}che zu Volumen (TPMS - Triply periodic minimal surface) auf. Des Weiteren zeigen die TPMS-Strukturen vorteilhafte Str{\"o}mungseigenschaften, die sowohl f{\"u}r die Beschichtung mit dem Katalysator-Material als auch die Durchstr{\"o}mung mit den Reaktionsmedien im Betrieb essentiell sind. So ist es beispielsweise m{\"o}glich, durch die Variation der Dimension einer TPMS-Struktur die Oberfl{\"a}che pro Volumeneinheit, den hydraulischen Durchmesser des Reaktors und somit auch den Transportprozess des Fluids deutlich zu verbessern. Diese Faktoren erm{\"o}glichen eine effektivere Gas-Katalysator-Reaktion. Im Vergleich zu Mikroreaktorstrukturen aus den traditionellen Herstellungsverfahren liefern die additiv gefertigten Strukturen sowohl eine h{\"o}here CO2-Umwandlungsrate als auch eine CH4-Selektivit{\"a}t innerhalb des diffusionskontrollierten Bereichs.}, language = {de} } @misc{KotlarskiOrmanovaNikitinetal., author = {Kotlarski, Georgi and Ormanova, Maria and Nikitin, Alexander and Morozova, Iuliia and Ossenbrink, Ralf and Michailov, Vesselin and Doynov, Nikolay and Valkov, Stefan}, title = {Structure Formation and Mechanical Properties of Wire Arc Additively Manufactured Al4043 (AlSi5) Components}, series = {Metals}, volume = {14}, journal = {Metals}, number = {2}, issn = {2075-4701}, doi = {10.3390/met14020183}, abstract = {In the current paper, the correlation between the physical size of additively built wire arc specimens and their structure and properties is studied. For the purpose of this work, two oval shaped specimens of different lengths were manufactured under the same technological conditions. The specimens have a length of 200 mm and 400 mm and will be referred to as L200 and L400. The microstructure of the samples was studied using X-ray diffraction analysis (XRD), optical microscopy, and scanning electron microscopy (SEM). The microhardness, yield strength (YS), and ultimate tensile strength (UTS) were determined and their correlation with the technological conditions of specimen build-up was clarified. The results of the carried out experiments indicated that the crystallographic structure of both specimens is similar. The scanning electron microscopy images show a higher concentration of irregularly shaped micro-pores formed near the edge of the αAl grains in the structure of the L400 specimen compared to the L200 one. An increase in the size of the αAl solid solution grains in the case of the L200 specimen towards its top section was noticed using optical microscopy. A slightly lower magnitude change was noticed concerning the L400 specimen. The increase in the size of the aluminum crystals was determined to be the increasing interpass temperature. Due to the much smaller thermal dissipation capacity of the smaller specimen, the interpass temperature of the same increased faster compared to the larger specimen. All of the above-mentioned factors led to a decrease in the microhardness of the specimens at higher stages of build-up. Since the specimens were deposited using similar layer deposition conditions, the resultant YS and UTS data are also highly comparable.}, language = {en} } @misc{MiahKloshekOssenbrinketal., author = {Miah, Kamal Uddin Mohammad and Kloshek, Alexander and Ossenbrink, Ralf and Seidlitz, Holger}, title = {Selective Laser Melting of Pure Copper (Cu-ETP)}, series = {4th Symposium on Materials and Additive Manufacturing, Additive 2024, 22. - 24. Mai 2024, Book of Abstracts}, journal = {4th Symposium on Materials and Additive Manufacturing, Additive 2024, 22. - 24. Mai 2024, Book of Abstracts}, publisher = {Deutsche Gesellschaft f{\"u}r Materialkunde (DGM) e.V.}, address = {Bremen, Berlin}, isbn = {978-3-88355-440-2}, pages = {19}, abstract = {The main objective of this study is to address the difficulties related to the production of highly dense parts utilizing pure Cu-ETP powder. In order to achieve this goal, the SLM machine was modified by replacing the regular infrared laser with a laser operating in the range of 530 to 534 nm. Following this modification, a detailed experiment was conducted to determine the most effective procedural parameters for producing solid components and gyroid structures of Cu-ETP. The study determined thtat in order to produce a part density of 99.6 ± 0.2\%, the following parameters are required: a laser power of 130 ± 10 W, a scanning speed of 350 mm/s, and a layer thickness of 25 µm. The microscopic analysis on the SLM-manufactured components showed a consistent grain structure across the build parts. Furthermore, it was discovered that exceeding the predetermined laser power and scanning speed parameters led to lower density of the parts. Conversely, decreasing the laser power and scanning speed below these thresholds was determined to be economically disadvantageous.}, language = {en} } @misc{KehmWasilewskiMiahetal., author = {Kehm, Christian and Wasilewski, Eric and Miah, Kamal Uddin Mohammad and Ossenbrink, Ralf and Seidlitz, Holger}, title = {Effects of extended shielding gas coverage on component contour accuracy in Wire Arc Additive Manufacturing}, series = {4th Symposium on Materials and Additive Manufacturing, Additive 2024, 22. - 24. Mai 2024, Book of Abstracts}, journal = {4th Symposium on Materials and Additive Manufacturing, Additive 2024, 22. - 24. Mai 2024, Book of Abstracts}, publisher = {Deutsche Gesellschaft f{\"u}r Materialkunde (DGM) e.V.}, address = {Bremen, Berlin}, isbn = {978-3-88355-440-2}, pages = {29}, abstract = {Producing near-net-shape components with Wire Arc Additive Manufacturing (WAAM) is a challenging task. Compared to laser-based additive manufacturing technologies, WAAM is characterized by a lower contour accuracy with higher surface roughness and more uneven surface profiles. Therefore, the WAAM requires a high degree of post-processing (machining) which reduces economic efficiency and increases material consumption. Therefore, topics such as process optimization with regard to the component contour are increasingly in the focus of research. This study presents the application of an extended shielding gas coverage in the WAAM process of steel to improve part contour accuracy. A specially adapted shielding gas coverage was manufactured with laser powder bed fusion and following used to study the influence on the resulting component contour and properties in comparison to standard shielding gas nozzles. The investigations include the analysis of temperature profiles, shape deviations, hardness and porosity in the component. In addition, process parameters such as gas flow rate and nozzle geometry were varied in order to evaluate their influence on the accuracy of the component contour. The extended shielding gas coverage reduces the average deviation from the target contour significantly by a degree of 49,44\%. In addition, the maximum of the occurring deviation height could be decreased by 42,39\%. The results show an improvement in the dimensional accuracy of the contour and the surface quality, resulting in higher reproducibility and less post-processing effort.}, language = {en} } @misc{NikitinTurabovErmilovaetal., author = {Nikitin, Alexander and Turabov, Dashqin and Ermilova, Evgeniia and Evdokimov, Anton and Ossenbrink, Ralf and Seidlitz, Holger}, title = {Using dynamic resistance to predict electrode surface degradation in resistance spot welding of 5182 aluminum alloy}, series = {Welding in the World}, volume = {69}, journal = {Welding in the World}, doi = {10.1007/s40194-024-01872-9}, pages = {449 -- 458}, abstract = {In this study, the correlation between dynamic resistance during the first 10 ms of welding time and the electrode surface condition in resistance spot welding of 5182 aluminum alloy has been investigated. The electrode surface rapidly degrades due to contamination and morphological changes, adversely affecting the weld spot surface. The accumulation of Cu-Al intermetallic phases on the electrode surface alters its roughness, leading to variations in dynamic resistance. By analyzing this correlation, optimal electrode milling intervals were identified to extend electrode life. This work focused on detecting crater formation on the electrode surface through dynamic resistance monitoring. The results indicate that resistance measurements provide a reliable approach for evaluating electrode wear, optimizing maintenance schedules, and reducing material removal during milling.}, language = {en} } @misc{OrmanovaKotlarskiKaishevaetal., author = {Ormanova, Maria and Kotlarski, Georgi and Kaisheva, Darina and Nikitin, Alexander and Ossenbrink, Ralf and Doynov, Nikolay and Valkov, Stefan}, title = {Investigation of the thermal gradients formed during the process of cooling of WAAM built Al99.7 specimen}, series = {Journal of Physics: Conference Series}, volume = {2024}, journal = {Journal of Physics: Conference Series}, number = {2710}, issn = {1742-6596}, doi = {10.1088/1742-6596/2710/1/012038}, abstract = {This work presents a preliminary experiment used to determine the possibility of developing a thermal model used to predict the thermal gradients formed during the process of wire and arc additive manufacturing (WAAM). For this purpose, an Al99.7 specimen was built using gas metal arc welding (GMAW) in the cold arc pulse mode. The temperature of both the substrate and each consecutive layer was measured using thermocouples and infrared thermometers and the experimental data was used for the calibration of the developed thermal model. The obtained results can be used for the further development of the thermal model.}, language = {en} } @misc{KotlarskiOrmanovaNikitinetal., author = {Kotlarski, Georgi and Ormanova, Maria and Nikitin, Alexander and Ossenbrink, Ralf and Doynov, Nikolay and Valkov, Stefan and Michailov, Vesselin}, title = {Structure, morphology and hardness of a WAAM built Al99.7 specimen}, series = {International Scientific Conference Unitech 2023, Gabrovo : selected papers}, volume = {2}, journal = {International Scientific Conference Unitech 2023, Gabrovo : selected papers}, editor = {Tsankov, Plamen and Maximov, Jordan and Aleksandrov, Anatoliy and Todorov, Todor and Peneva, Petya}, publisher = {Union of Automation \& Informatics}, address = {Gabrovo}, issn = {1313-230X}, doi = {10.70456/PJKY7011}, pages = {349 -- 353}, abstract = {The present work discusses the possibility of wire arc additive manufacturing (WAAM) of pure aluminum specimens (Al99.7). The manufactured specimen's structure was studied using X-ray diffraction (XRD) experiments. The morphology of the specimen at different stages of build-up was studied by examining prepared mechanical properties of the specimen, and for this reason the microhardness of the specimen was studied as well. The results of the present study were discussed regarding the change of the structure of the samples with the increase of the specimen's height during the manufacturing process and its influence on the resultant microhardness.}, language = {en} } @misc{BergDueckershoffHertrampfetal., author = {Berg, Heinz Peter and D{\"u}ckershoff, Roland and Hertrampf, Stefan and Kloshek, Alexander and Himmelberg, Axel}, title = {Development of an injector spark plug for the injection and ignition of gaseous fuels in internal combustion engines for use in conventional systems}, series = {AIP Conference Proceedings}, volume = {3626 (2024)}, journal = {AIP Conference Proceedings}, publisher = {AIP Publishing}, address = {Chiang Mai}, doi = {10.1063/5.0238165}, pages = {1 -- 8}, abstract = {An injection-ignition-system from an additive manufacturing process is presented with which gaseous fuels can be injected into the combustion chamber of an internal combustion engine under pressures of up to 80 bar and ignited. With the presented system, an improvement of the thermal efficiency can be achieved by a late fuel injection in the compression phase and with post-injection. With such a system, the engine becomes purely air-intake and a better filling level is achieved. Injection and ignition can take place simultaneously with this application. The system is designed with a high pressure stability for all components (200 bar) and can therefore also be used with higher compressions and combustion pressures. The spatial distribution of the fuel in the combustion chamber is achieved by angled fluid ports and also allows additional injections and ignitions in the power stroke and in the relief phase. This can improve thermal efficiency. A built-in annular channel also enables two different fuels to be injected as a mixing chamber. Finally, initial measurement results are shown for the use of hydrogen fuel in a single-cylinder engine. Indexing data and performance data of the engine indicate that the system can represent a significant increase in the efficiency of combustion engines with hydrogen fuel. Furthermore, the system can be used in conventional vehicle systems, whereby only fuel conditioning and control systems need to be adapted.}, language = {en} } @misc{FlorianSchrickerZenzetal., author = {Florian, Tobias and Schricker, Klaus and Zenz, Constantin and Otto, Andreas and Schmidt, Leander and Diegel, Christian and Friedmann, Hannes and Seibold, Marc and Hellwig, Peter and Fr{\"o}hlich, Fabian and Nagel, Falk and Kallage, Peter and Buttazzoni, Michele and Rack, Alexander and Requardt, Herwig and Chen, Yunhui and Bergmann, Jean Pierre}, title = {Combining in situ synchrotron X-ray imaging and multiphysics simulation to reveal pore formation dynamics in laser welding of copper}, series = {International Journal of Machine Tools and Manufacture}, volume = {204}, journal = {International Journal of Machine Tools and Manufacture}, publisher = {Elsevier BV}, issn = {0890-6955}, doi = {10.1016/j.ijmachtools.2024.104224}, pages = {1 -- 22}, abstract = {Laser beam welding has emerged as a powerful tool for manufacturing copper components in electrical vehicles, electronic devices or energy storage, owing to its rapid processing capabilities. Nonetheless, the material's high thermal conductivity and low absorption of infrared light can introduce process instabilities, resulting in defects such as pores. This study employs a hybrid approach that combines in situ synchrotron X-ray imaging with compressible multiphysics process simulation to elucidate pore-forming mechanisms during laser beam welding of copper. High-speed synchrotron X-ray imaging with an acquisition rate of 20,000 images/second facilitates the identification of relevant process regimes concerning pore formation during laser beam welding of copper with a wavelength of 1070 nm. Furthermore, in situ observations with high temporal and spatial resolution present a unique database for extensive validation of a multi-physics process simulation based on welding processes using different concentric intensity distributions. These validated simulation results enable thorough comprehension of process-related pore formation based on the interaction between keyhole, melt pool and resulting flow field. The findings show that pore formation is driven by four different mechanisms: bulging, spiking, upwelling waves at the keyhole rear wall and melt pool ejections. The synergy of high- speed synchrotron X-ray imaging and multi-physics modeling provides a fundamental understanding of the chronological sequence of events leading to process-related pore formation during laser beam welding of copper.}, language = {en} } @misc{KoehlerNikitinSonnenfeldetal., author = {K{\"o}hler, Marcel and Nikitin, Alexander and Sonnenfeld, Peter and Ossenbrink, Ralf and J{\"u}ttner, Sven}, title = {Wire arc additive manufacturing of aluminum foams using TiH2-Laced Welding Wires}, series = {Materials}, volume = {17}, journal = {Materials}, number = {13}, publisher = {MDPI AG}, issn = {1996-1944}, doi = {10.3390/ma17133176}, abstract = {Composite materials made from aluminum foam are increasingly used in aerospace and automotive industries due to their low density, high energy absorption capacity, and corrosion resistance. Additive manufacturing processes offer several advantages over conventional manufacturing methods, such as the ability to produce significantly more geometrically complex components without the need for expensive tooling. Direct Energy Deposition processes like Wire Arc Additive Manufacturing (WAAM) enable the additive production of near-net-shape components at high build rates. This paper presents a technology for producing aluminum foam structures using WAAM. This paper's focus is on the development of welding wires that are mixed with a foaming agent (TiH2) and produce a foamed weld metal as well as their processing using MIG welding technology.}, language = {en} }